Abstract:In this paper, the preparation and experimental diagnostic of low-pressure and low-temperature non-equilibrium plasma in industrial production and military applications are investigated. A one-dimensional fluid model of capacitive coupled RF plasma discharge is established by using the COMSOL software plasma module. The axial distribution of electron number density and electron temperature under different pressures and different voltages are calculated taking Helium as working gas. The electron density ne and electron temperature Te are also calculated according to the equivalent circuit of uniform RF discharge by building a plasma generation and diagnosis platform. The results show that when the gas pressure is 100~250Pa, the electron density increases first and then decreases along the axis, the electron temperature reaches the minimum at the center of the electrodes. There are two peaks in the edge of the electrodes, and the average electron temperature is only a function of the pressure and the size of the cavity. With the increase of input power, the electron density increases from gradually to rapidly, and this jump of electron density appears in different voltage amplitudes at different pressures, which indicates the α -γ transition in capacitively coupled discharge. The experimental diagnostic is consistent with the results of COMSOL simulation. The conclusions expand the application range of simulation and experiment for fast non-interference diagnosis, which is useful for further study on low-temperature plasma discharge.
[1] 戴栋, 宁文军, 邵涛. 大气压低温等离子体的研究现状与发展趋势[J]. 电工技术学报, 2017, 32(20): 1-9. Dai Dong, Ning Wenjun, Shao Tao.A review on the state of art and future trends of atmospheric pressure low temperature plasmas[J]. Transactions of China Electrotechnical Society, 2017, 32(20): 1-9. [2] 张晓星, 肖焓艳, 黄杨珏. 低温等离子体处理SF6废气综述[J]. 电工技术学报, 2016, 31(24): 16-24. Zhang Xiaoxing, Xiao Hanyan, Huang Yangyu.A review of degradation of SF6 waste by low temperature plasma[J]. Transactions of China Electrotechnical Society, 2016, 31(24): 16-24. [3] 林浩凡, 王瑞雪, 谢庆, 等. 等离子体射流快速改性促进表面电荷衰减[J]. 电工技术学报, 2017, 32(16): 256-264. Lin Haofan, Wang Ruixue, Xie Qing, et al.Rapid surface modification by plasma jet to promote surface charge decaying[J]. Transactions of China Electro- technical Society, 2017, 32(16): 256-264. [4] 程显, 徐晖, 王瑞雪, 等. 等离子体复合薄膜沉积抑制金属微粒启举[J]. 电工技术学报, 2018, 33(20): 4672-4681. Cheng Xian, Xu Hui, Wang Ruixue, et al.Composite thin film deposited by plasma to inhibit the lifting of metal particles[J]. Transactions of China Electro- technical Society, 2018, 33(20): 4672-4681. [5] Hwang S W, Lee H, Lee H J.Effect of electron Monte Carlo collisions on a hybrid simulation of a low-pressure capacitively coupled plasma[J]. Plasma Sources Science and Technology, 2014, 23(6): 65040. [6] Kim D H, C M Ryu. Particle simulation of a magnetically enhanced dual-frequency capacitively coupled plasma[J]. Journal of Physics D: Applied Physics, 2008, 41(1): 015207. [7] 熊路遥. 容性耦合放电的PIC模型[D]. 上海: 东华大学, 2017. [8] 杨旺, 刘学平, 夏焕雄, 等. 容性耦合等离子体腔室放电特性仿真研究[J]. 真空科学与技术学报, 2015, 35(6): 639-645. Yang Wang, Liu Xueping, Xia Huanxiong, et al.Simulation of discharge characteristics of capaci- tively coupled plasma[J]. Chinese Journal of Vacuum Science and Technology, 2015, 35(6): 639-645. [9] Chen Guangye, Raja L L.Fluid modeling of electron heating in low-pressure, high-frequency capacitively coupled plasma discharges[J]. Journal of Applied Physics, 2004, 96(11): 6073-6081. [10] Bukowski J D, Graves D B, Vitello P.Two dimensional fluid model of an inductively coupled plasma with comparison to experimental spatial profiles[J]. Journal of Applied Physics, 1996, 80(5): 2614. [11] 刘冲, 何湘, 张亚春, 等. 射频容性耦合等离子体放电特性的光谱诊断[J]. 光谱学与光谱分析, 2018, 38(4): 1007-1013. Liu Chong, He Xiang, Zhang Yachun, et al.Spectro- scopic diagnostics on discharge characteristics RF capacitively coupled plasma[J]. Spectroscopic and Spectral Analysis, 2018, 38(4): 1007-1013. [12] Kechkar S, Swift P, Kelly S, et al.Investigation of the electron kinetics in O2 capacitively coupled plasma with the use of a Langmuir probe[J]. Plasma Sources Science and Technology, 2017, 26(6): 065009. [13] 林敏, 徐浩军, 苏晨, 等. 低气压闭式等离子体放电实验及光谱诊断[J]. 光谱学与光谱分析, 2014, 34(6): 1594-1598. Liu Min, Xu Haojun, Su Chen, et al.Experim entalstudy on closed plasma discharging under low pressure and spectroscopic diagnosis[J]. Spectro- scopic and Spectral analysis, 2014, 34(6): 1594-1598. [14] Godyak V A.Soviet radio frequency discharge research[M]. Valery A: Delphicus, 1986: 28-52. [15] Li S Z, Lim J P, Uhm H S.Discharge characteristics of an atmospheric-pressure capacitively coupled radio-frequency argon plasmas[J]. Physics Letters A, 2006, 360(2): 304-308. [16] 王宇天, 张百灵, 李益文, 等. 基于均匀模型的低气压电容耦合射频放电特性研究[J]. 真空科学与技术学报, 2016, 36(7): 773-778. Wang Yutian, Zhang Bailing, Li Yiwen, et al.Modeling and characterization of low-pressure capacitive coupled RF discharge properties[J]. Chinese Journal of Vacuum Science and Technology, 2016, 36(7): 773-778. [17] He Xiang, Liu Chong, Zhang Yachun, et al.Diagnostic of capacitively coupled radio frequency plasma from electrical discharge characteristics: comparison with optical emission spectroscopy and fluid model simulation[J]. Plasma Science and Technology, 2018, 20(2): 024005. [18] 夏亚龙, 林莘, 徐建源, 等. 非平衡态SF6等离子体弛豫特性研究[J]. 电工技术学报, 2018, 33(5): 1125-1132. Xia Yalong, Lin Xin, Xu Jianyuan, et al.Study on the relaxation characteristics of non-equilibrium SF6 plasma[J]. Transactions of China Electrotechnical Society, 2018, 33(5): 1125-1132. [19] 孙恺, 辛煜, 黄晓江, 等. 60MHz电容耦合等离子体中电子能量分布函数特性研究[J]. 物理学报, 2008(10): 6465-6470. Sun Kai, Xin Yu, Huang Xiaojiang, et al.Chara- cteristics of electron energy distribution function of capacitively coupled plasma excited[J]. Acta Physica Sinica, 2008(10): 6465-6470. [20] 索南加乐, 邓旭阳, 阿里木江·卡德尔, 等. 基于综合阻抗的母线保护新原理[J]. 电力系统保护与控制, 2010, 38(18): 1-7. Suo Nanjiale, Deng Xuyang, A Limujiangkadeer, et al. A novel principle of integrated impedance based bus-bar protection[J]. Power System Protection and Control, 2008, 38(18): 1-7. [21] Puač N, Petrović Z L, Radetić M, et al.Low pressure rf capacitively coupled plasma reactor for modi- fication of seeds, polymers and textile fabrics[J]. Materials Science Forum, 2005, 494: 291-296. [22] He Xiang, Chen Jianping, Ni Xiaowu, et al.Experi- mental and numerical investigation on electro- magnetic absorption and diffraction by the plasma- covered cavity[J]. IEEE Transactions on Plasma Science, 2011, 38(12): 3342-3347.